A record-breaking thermal desorption system comes home to Markes
Tuesday, 9 October 2018 at 4:07:PM
|On 8 October, we were delighted to welcome a special visitor to our UK Service Department in Llantrisant – Dr Swaraj Paul, founder of PP Polymer,
based near Stockholm, Sweden. As well as wanting to see the latest
instruments in our demo lab, Dr Paul had a more unusual reason for
visiting us – to bring along for a quick service his 19-year-old UNITY 1! || |
Dr Paul’s UNITY 1 thermal desorber – a piece of history!
A long-lived thermal desorption unit
The instrument (pictured right) is a piece of
Markes history, being the ninth TD unit Markes ever made, and sold to
him in 1999 by our co-founder Elizabeth Woolfenden. Perhaps its design
doesn’t quite compare to the sleek lines of our new UNITY-xr, but of
course what matters most is how well it works, and Dr Paul was pleased
to report that his instrument is still going strong!
Dr Paul told us that the team at PP Polymers use their UNITY
to analyse small samples of polymer, by desorbing them directly within a TD
tube, and analysing the vapours using GC–MS. The results they obtain provide
information on the composition of the polymer, which they use to help their
clients control product quality and improve consumer safety.
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Correlation to thermogravimetric analysis
Dr Paul said that the simplicity of direct desorption and
the straightforward controls of the UNITY allow them to generate reliable data
on VOC emissions, which is easy to correlate to the results of one of the other
methods they use, thermogravimetric analysis (TGA). This stands in contrast to
other more error-prone methods such as solvent extraction, which he said are
still widely used in the field of polymer analysis.
The UNITY was given a check-over to resolve a leak by Arfon Jones, one of our
service team. Afterwards, Arfon commented “Although our UNITY 1 thermal
desorbers are now discontinued, we still have a considerable number of people
out there for whom the instrument does precisely the job it needs to, day-in,
day-out. It was a great pleasure to meet such a long-standing customer, and of
course to personally service the oldest Markes thermal desorber still in use!”.
Service Engineer Arfon Jones (left) and Dr Swaraj Paul (right) shaking hands on the next 19 years of successful instrument operation!
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David Barden received his Ph.D. in Organic Chemistry from Cambridge University in 2004, and during his time as an editor at the RSC wrote news pieces for Chemistry World on various scientific topics. He is now Technical Copywriter at Markes International, where he draws on the expertise of his colleagues to explain how thermal desorption and mass spectrometry technologies can be applied to analyse volatile organic compounds in a wide variety of situations.